HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → 2,6-Dichloro-3-nitroquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 6-Chloro-3-nitroquinoline-1-oxide | HCID 13472701 | — |
| Product | 2,6-Dichloro-3-nitroquinoline | HCID 13472702 | — |
Reaction Steps
2,6-Dichloro-3-nitroquinoline was prepared by heating a mixture of 6-chloro-3-nitroquinoline-1-oxide and phosphorous oxychloride under reflux. The product was isolated as a nearly colourless crystalline solid, mp 190° C. Mass spectrum (m/e): 242 (parent ion; 90%); 196 (100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04444584 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-33630359d8e44fc6baaecc2939e33573 |
| Source note | uspto-grants-1984_04 |