HuagongsheHuagongshe Chemistry Print Report · For research reference only
Quinoline → 4-[N-(6,8-dichloro-2-quinolinyl)-N-methylamino]-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Quinoline | HCID 7047 | — |
| Reactant | p-(N-methylamino)phenol sulfate | HCID 10198132 | — |
| Reactant | 2,6,8-Trichloroquinoline | HCID 20461944 | — |
| Product | 4-[N-(6,8-dichloro-2-quinolinyl)-N-methylamino]-phenol | HCID 20461934 | — |
Reaction Steps
4-[N-(6,8-dichloro-2-quinolinyl)-N-methylamino]-phenol was prepared from 2,6,8-trichloroquinoline and 4-(N-methylamino)phenol sulfate following essentially the same procedure as that described in Example 19, Part a). Proton magnetic resonance spectrum (CDCl3 ; δ in ppm): 8.0-6.6 and 7.1 (9H, m, and d of d, quinoline, OH and phenyl protons; 3.6 (3H, s, N--CH3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04444584 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-ab07c0e45df94df19a082206e0129f76 |
| Source note | uspto-grants-1984_04 |