HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octylamine → 1-octylazepan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octylamine | HCID 8143 | — |
| Reactant | epsilon-CAPROLACTONE | HCID 10401 | — |
| Product | 1-octylazepan-2-one | HCID 2754067 | 27% |
Reaction Steps
Following example 5, heating 17.5 g (0.153 M) of 6-hexanolactone and 22 g (0.17 M) of 1-aminooctane at 180° for 29 hr. gave 8.8 g (27%) of product; b.p. 155°-160°/0.5 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04444762 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-1822b2191a8749d6bffd6e7432ba2721 |
| Source note | uspto-grants-1984_04 |