HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 326203Generated: October 30, 2026
Thionyl Chloride → 5-Hexylthiophene-2-carboxylic acid chloride
https://huagongshe.com/reaction/326203
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-Hexyl-2-thiophenecarboxylic acid | HCID 13128269 | — |
| Product | 5-Hexylthiophene-2-carboxylic acid chloride | HCID 13128272 | — |
Reaction Steps
10 ml of thionyl chloride was added to 1.0 g (4.72×10-3 ml) of 5-hexylthiophene-2-carboxylic acid, followed by stirring for 4 hours under heating at 80° C. and removal of excessive thionyl chloride by reduced-pressure distillation to obtain 5-hexylthiophene-2 -carboxylic chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05268123 |
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| Source dataset | uspto-grants-1993_12 |
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| ORD ID | ord-428139fe7d494ec893429a8e138d97bd |
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| Source note | uspto-grants-1993_12 |
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