HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonate → 4-Methoxy-4-(3-methanesulfonyl-trans-prop-1-enyl)tetrahydropyran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonate | HCID 85257 | — |
| Reactant | 4-Methoxy-4-(3-hydroxy-trans-prop-1-enyl)tetrahydropyran | HCID 15199064 | — |
| Product | 4-Methoxy-4-(3-methanesulfonyl-trans-prop-1-enyl)tetrahydropyran | HCID 19388026 | — |
Reaction Steps
4-methoxy-4-(3-hydroxy-trans-prop-1-enyl)tetrahydropyran, prepared as in Example 3, was converted to the corresponding mesylate according to the method of Crossland and Servis, J. Org. Chem., 35, 3195-3196 (1970).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05268379 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-386fda5ed4944274bc1fd85f94b3224b |
| Source note | uspto-grants-1993_12 |