HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-dimethylamino-pyrimidine-5-carboxylic acid benzylamide → HCID 178418259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-dimethylamino-pyrimidine-5-carboxylic acid benzylamide | HCID 53723042 | — |
| Reactant | Sodium hydrogen sulphide | HCID 86586439 | — |
| Product | HCID 178418259 | HCID 178418259 | 43.9% |
Reaction Steps
Using the procedure of Preparation 34, 14.3 g (0.045 mol) of 4-chloro-2-dimethylamino-pyrimidine-5-carboxylic acid benzylamide and 12 g (0.21 mol) of sodium hydrogen sulfide were reacted to give 5.7 g of the title compound, mp 175°-178° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05733921 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-1bfad829bc4246f8aaa002d4fbd32d86 |
| Source note | uspto-grants-1998_03 |