Hydrochloric Acid → HCID 19735229, compound

Participants

Reaction Steps

To a solution of N,N-diethyl-N'-hexadecanoyl-1,3-propanediamine (10.9 g, 29.6 mmole) in diethyl ether was added an ethereal solution of hydrogen chloride. The reaction mixture was placed in the refrigerator overnight. The precipitate was filtered to give the title compound (8.60 g, 65%) as a pasty solid. 1H NMR (300 MHz, CDCl3): δ0.855 (3H, t, J=6.7 Hz), 1.229 (24H, bs), 1.367 (3H, bs), 1.626 (2H, bs), 2.08 to 2.10 (2H, m), 3.153 (6H, bs), 3.414 (2H, bs), and 6 32 to 6.36 (1H, bs). Analysis calculated for C23H46N2O.1.4 HCl.1.5 H2O: C, 62.12; H, 11.42; N, 6.29; Cl, 11.16. Found: C, 62.50; H, 11.52; N, 6.31; Cl, 11.28.

Provenance & Evidence