Hydrochloric Acid → HCID 19735240, compound

Participants

Reaction Steps

To a solution of N,N-dimethyl-N'-hexadecanoyl-N'-propyl-1,3-propanediamine (2.78 g, 6.94 mmole) in diethyl ether was added an ethereal solution of hydrogen chloride. The reaction mixture was placed in the refrigerator overnight. The precipitate was filtered to give the title compound (2.01g, 63%) as a paste. 1H NMR (300 MHz, CDCl3): δ0.83 to 0.93 (6H, m), 1.232 (24H, bs), 1.54 to 1.69 (4H, m), 2.00 to 2.20 (2H, m), 2.288 (2H, t, J=7.5 Hz), 2.788 (3H, s), 2.803 (3H, s), 2.95 to 3.10 (2H, m), 3.225 (2H, t, J=7.7 Hz), and 3.401 (2H, t, J=6.7 Hz). IR (neat): 2917, 2848, 1633, and 1172 cm-1. Analysis calculated for C24H50N2O.3/4HCl.1.2H2O: C, 65.52; H, 12.07; N, 6.36; Cl, 9.67. Found: C, 65.51; H, 11.98; N, 6.36; Cl, 9.73.

Provenance & Evidence