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HRID32667

反应详情

EQUATION

反应方程式

HRID 32667 的结构方程式

REACTANTS

反应物

3
结构：CC(C)I
HCID6362

2-Iodopropane

C3H7I

结构：CS(=O)(=O)c1ccc(Cl)c(C(=O)O)c1
HCID2329132

2-chloro-5-(methylsulfonyl)benzoic acid

C8H7ClO4S

结构：O=C(O)c1cc(S(=O)O)ccc1Cl
HCID15112904

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)S(=O)(=O)c1ccc(Cl)c(C(=O)O)c1
HCID43140999

未命名化合物

收率 42%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The title compound was synthesised according to the procedure described for the synthesis of 2-Chloro-5-methanesulfonyl-benzoic acid from 2-Chloro-5-sulfino-benzoic acid and 2-iodopropane in 20 ml water and obtained in 42% yield. MS (m/e): 261.1 (MH−, 100%).

WORKUP

后处理

  1. customobtained in 42% yield