HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 326758Generated: October 30, 2026
1-Bromo-2-nitrobenzene → 4'-Methyl-2-nitro-1,1'-biphenyl
https://huagongshe.com/reaction/326758
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Bromo-2-nitrobenzene | HCID 11341 | — |
| Reactant | 4-Iodotoluene | HCID 12207 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4'-Methyl-2-nitro-1,1'-biphenyl | HCID 10443194 | — |
Reaction Steps
11.2 g of 2-nitrobromobenzene are mixed with 15 g of 4-iodotoluene and the mixture is heated to 195° C. and stirred at this temperature for 3 and a half hours. After returning to room temperature, it is taken up in DCM and heated to the reflux point, the hot solution is filtered on Celite® and the DCM is then evaporated off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05270317 |
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| Source dataset | uspto-grants-1993_12 |
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| ORD ID | ord-40fe96446dfb4f2b9b7a0a614b918bb6 |
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| Source note | uspto-grants-1993_12 |
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