HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54280592, compound → HCID 53843061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54280592 | HCID 54280592 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Reactant | HCID 178418443 | HCID 178418443 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 53843061 | HCID 53843061 | 44% |
Reaction Steps
In a similar manner as Example 62 except for using 18 ml of a solution of 1.6M n-butyllithium in hexane instead of 10 ml of the solution of 3N ethyl magnesiumbromide in THF for reacting with 3-(m-phenoxybenzylidene)-1-pyrroline, 3.2 g (yield 44%) of 2-n-butyl-3-(m-phenoxybenzylidene)-pyrrolidine was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270339 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-c19b8862765a480cadd55b07bc69a2a3 |
| Source note | uspto-grants-1993_12 |