HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 178467657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3-Amino-5-oxo-4,5-dihydropyrazine-2-carboxamide | HCID 178513807 | — |
| Solvent | N,N-dimethylformamide methanol | HCID 21901440 | — |
| Product | HCID 178467657 | HCID 178467657 | — |
Reaction Steps
Obtained using the procedure described in Example 1, starting with 2.1 g (0.0136 mole) of 3-amino-5-hydroxy-2-pyrazinecarboxamide [prepared according to E. C. Taylor et al., J. Org. Chem. 1975, 40, 2341], 14.0 g (0.068 mole) of triethyl orthoethoxyacetate and 14.0 ml of acetic anhydride. Yld: 1.2 g (40%), m.p. 255°-256° C. (methanol/N,N-dimethylformamide).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270465 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-e03ba369b974429d9cdf4d031c4e1528 |
| Source note | uspto-grants-1993_12 |