HRID326841

反应详情

EQUATION

反应方程式

HRID 326841 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Obtained using the procedure described in section c of Example 2, starting with 12.0 g (0.10 mole) of 3-amino-2-pyrazinecarbonitrile and 18.0 g (0.15 mole) of 2-(methoxymethoxy)acetamidine in 400 ml of absolute ethanol. Refluxing time: 4 hours. Yld: 15.8 g (71%), m.p. 129°-131° C. (ethanol).

WORKUP

后处理

  1. customObtained
  2. temperatureRefluxing time
  3. custom4 hours