Ammonia → HCID 3638364, compound

HRID 326852Notes

Reaction equation

HRID 326852 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:11]=[CH:12][C:13]=1[Cl:14])[O:5][CH2:6][C:7](=[NH:10])OC.[NH3:15]>C(O)C>[Cl:1][C:2]1[CH:3]=[C:4]([CH:11]=[CH:12][C:13]=1[Cl:14])[O:5][CH2:6][C:7]([NH2:15])=[NH:10]

Participants

4

Reactant 2

HCID 222AmmoniaHCID 10752137HCID 10752137, compound

Product 1

HCID 3638364HCID 3638364, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Obtained using the procedure described in section b of Example 2, starting with 28.2 g (0.12 mole) of methyl 2-(3,4-dichlorophenoxy)acetimidate and 10.2 g (0.60 mole) of ammonia in 480 ml of absolute ethanol. Reaction time: 3 hours. Yld: 26.3 g (quantitative).

Workup

  1. customObtained
  2. customReaction time
  3. custom3 hours

Sources & evidence

ORD record
ord-a30eb051d6364feead6fa1f5119b0dc3
Source dataset
uspto-grants-1993_12
Patent number
US05270465

Reaction notes

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