HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Amino-3-nitrobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Amino-3-nitrobenzoic acid | HCID 219633 | — |
| Product | 2-Amino-3-nitrobenzoyl chloride | HCID 21251967 | 100% |
Reaction Steps
A mixture of 9.90 parts of 2-amino-3-nitrobenzoic acid and 32.4 parts of thionyl chloride was stirred for 15 min at reflux temperature under argon. The excess of thionyl chloride was evaporated, yielding 10.8 parts (100%) of 2-amino-3-nitrobenzoyl chloride (interm. 39).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270464 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-2efa173836474511a5a4f86436526802 |
| Source note | uspto-grants-1993_12 |