HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetic Acid → Octyl bromoacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetic Acid | HCID 6227 | — |
| Reactant | 1-Decanol | HCID 8174 | — |
| Catalyst | p-Toluenesulfonic acid | HCID 6101 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Octyl bromoacetate | HCID 347413 | 117.4% |
Reaction Steps
20 g of bromoacetic acid, 22 g of n-decyl alcohol, and 2.5 g of p-toluenesulfonic acid were added to 150 ml of toluene, and the azeotropic dehydration was carried out for 1.5 hours. After cooling the mixture by allowing it to stand, the toluene was removed under reduced pressure and then vacuum distillation was performed, to obtain 41 g of n-octyl bromoacetate (121° C., 10 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05272050 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-2fd91b61bc064e369c0264cdf84b2229 |
| Source note | uspto-grants-1993_12 |