HCID 67809871, compound → HCID 131718273, compound

Participants

Reaction Steps

In a vial, add ethanol (1 ml) to the product of Example 100 (0.050 g) and add PtO (0.025 g). Place a balloon filled with H2 gas over the mouth of the vial and stir overnight. Purify the resultant product on a silica column, eluting with CH2Cl2 →5% methanol/CH2Cl2. Add 0.1 N HCl (2 ml) to the resulting product and lyophilize to obtain the title compound, MS: m/z 339 (M+ +1).

Provenance & Evidence