HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Di-tert-butyl-4-mercaptophenol → 2,6-Di-tert-butyl-4-mercaptophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | Diethyl azodicarboxylate | HCID 5462977 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Product | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
Reaction Steps
Combine 3,5-di-t-butyl-4-hydroxythiophenol (751mg), diethylazodicarboxylate (496μL, 3.15mmol) and p-dioxane (5mL). Place under an argon atmosphere and stir for 2 hours to give a complex of 3,5-di-t-butyl-4-hydroxythiophenol and diethyl azodicarboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05272252 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-2d7f24b869d04191a8e5afc4fa6240d4 |
| Source note | uspto-grants-1993_12 |