HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-Bromoundecanoic acid → Undecanoyl chloride, 11-bromo-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-Bromoundecanoic acid | HCID 17812 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Undecanoyl chloride, 11-bromo- | HCID 85202 | — |
Reaction Steps
11-Bromoundecanoic acid (400 g) was added to thionyl chloride (600 ml) and the solution heated at 80° for 0.5 hour. The thionyl chloride was distilled off and the dark oily residue distilled in vacuo to give 11-bromoundecanoyl chloride, b.p. 144°, 0.7 mm Hg, (346.8 g, 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273740 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-6cf0c1ec3405470791493e943ea7bff2 |
| Source note | uspto-grants-1993_12 |