HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 8-bromooctanoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 8-Bromooctanoic acid | HCID 548275 | — |
| Product | 8-bromooctanoyl Chloride | HCID 11402228 | — |
Reaction Steps
8-Bromooctanoic acid (200 g) was added slowly to thionyl chloride (325 ml). The mixture was stirred at 60° for 1 hour. Excess thionyl chloride distilled off in vacuo. The dark oily residue was distilled to give 8-bromooctanoyl chloride as colorless oil, b.p. 112°-114°/0.1-0.3 mm Hg, (202.38, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273740 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-c2c46ba0ffbf4f4dafe406546b36d248 |
| Source note | uspto-grants-1993_12 |