1,2-Difluoro-3-(octyloxy)benzene → 4-n-Octyloxy-4"-n-pentyl-2,3-difluoro-p-terphenyl

HRID 327369Notes

Reaction equation

HRID 327369 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])[C:3]=1[F:17].C(O[C:25]1[CH:30]=[CH:29][C:28](Br)=[C:27](F)[CH:26]=1)CCCCC>>[CH2:9]([O:8][C:4]1[CH:5]=[CH:6][C:7]([C:2]2[CH:7]=[CH:6][C:5]([C:25]3[CH:26]=[CH:27][C:28]([CH2:9][CH2:10][CH2:11][CH2:12][CH3:13])=[CH:29][CH:30]=3)=[CH:4][CH:3]=2)=[C:2]([F:1])[C:3]=1[F:17])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 105624971,2-Difluoro-3-(octyloxy)benzeneHCID 191078664-n-Hexyloxy-2-fluorobromobenzene

Product 1

HCID 144957604-n-Octyloxy-4"-n-pentyl-2,3-difluoro-p-terphenyl

Procedure

This compound is prepared by an analogous route using 1,2-difluoro-3-octoxybenzene instead of 8B. This is prepared using the method as for 3A.

Workup

  1. customThis compound is prepared by an analogous route
  2. customThis is prepared

Sources & evidence

ORD record
ord-0039cc6b358c4a43943cde65b666c007
Source dataset
uspto-grants-1993_12
Patent number
US05273680

Reaction notes

Loading…