Iodoethane → HCID 11724054, compound

Participants

Reaction Steps

In 10 ml of ethanol were dissolved 0.8 g of 5-[3-(1-acetylpiperidin-4-yl)-1-oxopropyl]-2,3-dihydro-1H-indole, 2.1 g of ethyl iodide and 0.5 g of potassium carbonate and the solution was refluxed for 24 hours. The solid matter and the solvent were removed and the residue was purified by column chromatography (eluent: ethyl acetate: methanol=20:1) to give 0.85 g of the title compound as a pale yellow oil.

Provenance & Evidence