HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-bromo-1,2,3,4-tetrahydro-8-nitro-N,N-dipropyl-3-quinolinamine → 1,2,3,4-tetrahydro-N3,N3-dipropyl-3,8-quinolinediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-bromo-1,2,3,4-tetrahydro-8-nitro-N,N-dipropyl-3-quinolinamine | HCID 19919400 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1,2,3,4-tetrahydro-N3,N3-dipropyl-3,8-quinolinediamine | HCID 15291950 | 101.3% |
Reaction Steps
A mixture of 6-bromo-1,2,3,4-tetrahydro-8-nitro-N,N-dipropyl-3-quinolinamine (2.7 g) and 10% palladium charcoal (0.5 g) in ethanol (150 mL) was hydrogenated for 18 hours. The solution was filtered and the ethanol evaporated to give 1.9 g of 1,2,3,4-tetrahydro-N3,N3 -dipropyl-3,8-quinolinediamine as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273975 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-5096e36bf38d40bdada1cdf61f0a090e |
| Source note | uspto-grants-1993_12 |