HuagongsheHuagongshe Chemistry Print Report · For research reference only
O,O-Dipyridin-2-yl carbonothioate → 6-(Dimethylamino)-6,7-dihydro-5H-pyrido(1,2,3-de)-1.4-benzoxazin-3(2H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O,O-Dipyridin-2-yl carbonothioate | HCID 719784 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 1,2,3,4-tetrahydro-N3,N3-dipropyl-3,8-quinolinediamine | HCID 15291950 | — |
| Reactant | 1,2,3,4-tetrahydro-8-hydroxy-N,N-dimethyl-3-quinolinamine | HCID 19919486 | — |
| Product | 6-(Dimethylamino)-6,7-dihydro-5H-pyrido(1,2,3-de)-1.4-benzoxazin-3(2H)-one | HCID 19919307 | — |
Reaction Steps
This compound was prepared by following the procedure of Example 56 part B, but substituting ethyl bromoacetate for di (2-pyridyl)thiocarbonate and the sodium salt of 1,2,3,4-tetrahydro-8-hydroxy-N,N-dimethyl-3-quinolinamine for 1,2,3,4-tetrahydro-N3,N3 -dipropyl-3,8-quinolinediamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273975 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-fb04c4b35c294851a2d2e2c2ab23edc9 |
| Source note | uspto-grants-1993_12 |