HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 19926181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-[(tert-Butoxycarbonyl)amino]-2-phenylpropanoic acid | HCID 2755992 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19926181 | HCID 19926181 | — |
Reaction Steps
N-(t-butoxycarbonyl)-2-phenyl-β-alanine was heated to reflux in acetone with benzyl bromide and potassium carbonate for 17 hours to yield DL-N-(t-butoxycarbonyl)-2-phenyl-β-alanine benzyl ester, m.p. 58°-59° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273982 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-a2e7c3882d454e31a25334b470fdb8ab |
| Source note | uspto-grants-1993_12 |