反应详情

The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 5-phenyl-1-pentanol. The oil obtained was further purified by chromatography using a column with methylene chloride as eluting agent. Evaporation of appropriate fractions gave a viscous oil which solidified on standing. The solid was recrystallized from ethyl ether-petroleum ether (bp range 30°-60° C.) to give the title compound as white solid, mp 63°-66° C. in 60% yield.

1. customThe oil obtained
2. customwas further purified by chromatography
3. washas eluting agent
4. customEvaporation of appropriate fractions
5. customgave a viscous oil which
6. customThe solid was recrystallized from ethyl ether-petroleum ether (bp range 30°-60° C.)