Chlorosulfamic acid → HCID 19733467, compound

HRID 327672Notes

Reaction equation

HRID 327672 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][O:7][C:8]1[CH:9]=[C:10]2[C:15](=[CH:16][CH:17]=1)[CH:14]=[C:13]([CH:18]([CH3:21])[CH2:19][OH:20])[CH:12]=[CH:11]2>>[S:1]([O:20][CH2:19][CH:18]([C:13]1[CH:12]=[CH:11][C:10]2[C:15](=[CH:16][CH:17]=[C:8]([O:7][CH3:6])[CH:9]=2)[CH:14]=1)[CH3:21])(=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 3334137414-52-1

Product 1

HCID 19733467HCID 19733467, compoundYield 21%

Procedure

The title compound was prepared by the procedure of Example 33 from sulfamoyl chloride and 2-(6-methoxy-2-naphthyl)propanol as white solid, mp 112°-115° C., in 21% yield.

Sources & evidence

ORD record
ord-3fedcedbf823410fa69652fbdd4d964b
Source dataset
uspto-grants-1993_12
Patent number
US05273993

Reaction notes

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