HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfamic acid → HCID 19108702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Reactant | 2-(3-Chlorophenoxy)ethanol | HCID 80270 | — |
| Product | HCID 19108702 | HCID 19108702 | 44% |
Reaction Steps
The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-(3-chlorophenoxy)ethanol. The oil obtained was further purified by chromatography and recrystallization as in Example 38 to give white solid, mp 66°-69° C., in 44% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273993 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-4e09f66b9a2d49faaf6f7141cc92bdc7 |
| Source note | uspto-grants-1993_12 |