Chlorosulfamic acid → HCID 19108675, compound

HRID 327677Notes

Reaction equation

HRID 327677 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Br:6][C:7]1[CH:16]=[CH:15][C:10]([O:11][CH2:12][CH2:13][OH:14])=[CH:9][CH:8]=1>>[S:1]([O:14][CH2:13][CH2:12][O:11][C:10]1[CH:15]=[CH:16][C:7]([Br:6])=[CH:8][CH:9]=1)(=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 991682-(p-Bromophenoxy)ethanol

Product 1

HCID 19108675HCID 19108675, compoundYield 69%

Procedure

The title compound was prepared by the procedures of Example 33 from sulfamoyl chloride and 2-(4-bromophenoxy)ethanol as white solid, mp 134°-137° C., in 69% yield.

Sources & evidence

ORD record
ord-4b1e6b4dc46f4a02b0e3af37aac63d8a
Source dataset
uspto-grants-1993_12
Patent number
US05273993

Reaction notes

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