HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2,4-Dichlorophenoxy)ethanol → 2-(2,4-Dichlorophenoxy)ethanol sulfamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2,4-Dichlorophenoxy)ethanol | HCID 8444 | — |
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Product | 2-(2,4-Dichlorophenoxy)ethanol sulfamate | HCID 19108689 | — |
Reaction Steps
The title compound was prepared by the procedures of Example 33 from sulfamoyl chloride and 2-(2,4-dichlorophenoxy)ethanol. The viscous oil obtained solidified and was recrystallized from isopropyl ether to give the solid title compound, mp 75°-77° C., in 35% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273993 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-1dee74034a374557bd1fb843cefa570e |
| Source note | uspto-grants-1993_12 |