3-Nitrophenol → HCID 10059221, compound

HRID 327701Notes

Reaction equation

HRID 327701 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([OH:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].Cl[S:12]([N:15]=C=O)(=[O:14])=[O:13]>C1(C)C=CC=CC=1>[N+:1]([C:4]1[CH:5]=[C:6]([O:10][S:12](=[O:14])(=[O:13])[NH2:15])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2]

Participants

4

Reactant 2

HCID 111373-NitrophenolHCID 70918Chlorosulfonyl isocyanate

Product 1

HCID 10059221HCID 10059221, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

This compound was prepared according to the procedure used in Example 84. A mixture of 13.9 g (0.1 mole) of 3-nitrophenol and 14.8 g (0.105 mole) of chlorosulfonyl isocyanate in 100 ml of toluene gave 16.9 g (78%) of tan flakes, mp 118°-120° C.

Workup

  1. customThis compound was prepared
  2. customgave 16.9 g (78%) of tan flakes, mp 118°-120° C.

Sources & evidence

ORD record
ord-bb5123ed00c349c299627fce47eb84f2
Source dataset
uspto-grants-1993_12
Patent number
US05273993

Reaction notes

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