HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)phenol → HCID 54414453, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)phenol | HCID 7376 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54414453 | HCID 54414453 | 88.8% |
Reaction Steps
This compound was prepared according to the procedure used in Example 84. A mixture of 18.4 g (0.114 mole) of α,α,α-trifluoro-m-cresol, 14.8 g (0.105 mole) of chlorosulfonyl isocyanate and 100 ml of toluene gave 22.5 g (82%) of a white solid, mp 100°-102° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273993 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-2ce77fa4fe664623a60d0389131b4102 |
| Source note | uspto-grants-1993_12 |