HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → 2-Chlorophenyl sulfamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 2-Chlorophenol | HCID 7245 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Benzene--cyclohexane (1/1) | HCID 18624872 | — |
| Product | 2-Chlorophenyl sulfamate | HCID 21694498 | 59% |
Reaction Steps
This compound was prepared by the procedure used in Example 84. A mixture of 12.8 g (0.1 mole) of 2-chlorophenol, 14.8 g (0.105 mole) of chlorosulfonyl isocyanate and 75 ml of toluene gave 12.2 g (59%) of the title compound as a white solid, mp 62.5°-63.5° C. (cyclohexane-benzene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273993 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-157f8010b822450ab1e80fe2343a03f8 |
| Source note | uspto-grants-1993_12 |