Benzene → HCID 50994329, compound

HRID 327720Notes

Reaction equation

HRID 327720 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[C:6]([Cl:8])[CH:7]=1.Cl[S:11]([N:14]=C=O)(=[O:13])=[O:12].C1C=CC=CC=1>C1(C)C=CC=CC=1>[Cl:1][C:2]1[CH:3]=[C:4]([O:9][S:11](=[O:13])(=[O:12])[NH2:14])[CH:5]=[C:6]([Cl:8])[CH:7]=1

Participants

5

Reactant 3

HCID 241BenzeneHCID 115713,5-DichlorophenolHCID 70918Chlorosulfonyl isocyanate

Product 1

HCID 50994329HCID 50994329, compoundYield 83%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The procedure used in Example 84 was used to prepare this compound from a mixture of 16.3 g (0.10 mole) of 3,5-dichlorophenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 75 ml of toluene. The compound was obtained in 83% yield as a white, fluffy solid, mp 146°-147° C. (benzene).

Workup

  1. customto prepare this compound

Sources & evidence

ORD record
ord-12bd3ea958994a1d93569d913b3b05d5
Source dataset
uspto-grants-1993_12
Patent number
US05273993

Reaction notes

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