HRID327725

反应详情

EQUATION

反应方程式

HRID 327725 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

This compound was prepared using the procedure of Example 84 from a mixture of 9.8 g (0.043 mole) of 3,5-bis(trifluoromethyl)phenol and 3.9 ml (0.095 mole) of chlorosulfonyl isocyanate in 50 ml of toluene. The solid product was recrystallized from benzene to yield 6.4 g (48%) of a pale yellow solid; mp 118°-120° C.

WORKUP

后处理

  1. customThis compound was prepared
  2. customThe solid product was recrystallized from benzene