反应详情

This compound was prepared according to the procedure used in Example 101. Thus, a mixture of 14.7 g (0.06 mole) of 2-(3-benzyloxyphenoxy)ethanol, 17 ml (0.066 mole) of sulfamoyl chloride (3.9M solution in acetonitrile) and 7.0 g (0.069 mole) of triethylamine in 150 ml of acetonitrile gave a viscous, oily residue. The oil was triturated with benzene-petroleum ether (30°-60° C.) and the solid was collected by filtration. The solid was recrystallized from chloroform to yield 8.6 g (44%) of a white solid, mp 107°-109° C.

1. customThis compound was prepared
2. customgave a viscous, oily residue
3. customThe oil was triturated with benzene-petroleum ether (30°-60° C.)
4. filtrationthe solid was collected by filtration
5. customThe solid was recrystallized from chloroform