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HRID32776

反应详情

EQUATION

反应方程式

HRID 32776 的结构方程式

REACTANTS

反应物

2
结构：CNC
HCID674

Dimethylamine

C2H7N

结构：CC(C)(C)OC(=O)N1CCN(c2ncnc(Cl)n2)CC1
HCID86600711

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1ncnc(N2CCN(C(=O)OC(C)(C)C)CC2)n1
HCID68903194

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of 2 mmol of 4-(4-Chloro-[1,3,5]triazin-2-yl)-piperazine-1-carboxylic acid tert-butyl ester in 15 ml of 2M dimethylamine in methanol was stirred at room temperature for 1 hour. Concentration and purification by chromatography (SiO2; ethyl acetate/cyclohexane 1:1) yielded the title compound as a colorless solid. MS (m/e): 309.1 (MH+, 100%)

WORKUP

后处理

  1. concentrationConcentration and purification by chromatography (SiO2; ethyl acetate/cyclohexane 1:1)