HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hexyn-1-ol → HCID 15117022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hexyn-1-ol | HCID 70234 | — |
| Reactant | 2-Bromobenzaldehyde | HCID 81129 | — |
| Product | HCID 15117022 | HCID 15117022 | 59.4% |
Reaction Steps
Using the procedure of example 5 and starting with 11.1 g (60 mmol) of 2-bromobenzaldehyde and 7.62 g (77 mol) of 5-hexyn-1-ol, 2-(6-hydroxy-1-hexynyl)benzaldehyde was obtained in 59.4% yield, as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273999 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-9085f39cd52d4765a9a1c35d29383d1a |
| Source note | uspto-grants-1993_12 |