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HRID 327968作成日:2026年10月26日

Acetic acid, 2-(triphenylphosphoranylidene)-, methyl ester → (E)-3-[3-[[5-(Acetyloxy)pentyl]oxy]phenyl]-2-propenoic Acid Methyl Ester

https://huagongshe.com/reaction/327968

反応式

関与物質

役割名称HCID仕込み量
反応物Acetic acid, 2-(triphenylphosphoranylidene)-, methyl esterHCID 17453—
反応物3-[[5-(Acetyloxy)pentyl]oxy]benzaldehydeHCID 19922110—
生成物(E)-3-[3-[[5-(Acetyloxy)pentyl]oxy]phenyl]-2-propenoic Acid Methyl EsterHCID 6778003180%

反応手順

Using the procedure of example 28, the title compound was prepared in 80% yield, from 2.6 g (10.4 mmol) of 3-[[5-(acetyloxy)pentyl]oxy]benzaldehyde and 4.0 g (12 mmol) of methyl (triphenylphosphoranylidene)acetate, as a colorless solid, mp 65°-67° C.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05273999
出典データセットuspto-grants-1993_12
ORD IDord-c8004816dd8c4c1d97d0f74f3500c462
出典メモuspto-grants-1993_12