HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67780168, compound → HCID 53695873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67780168 | HCID 67780168 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53695873 | HCID 53695873 | 97% |
Reaction Steps
Rac-(E)-6-[2-(3-methoxy-3-oxo-1-propenyl)-3-[6-[(tetrahydro-2H-pyran-2-yl)oxy]-1-hexynyl]phenyl]-5-hexynoic acid methyl ester from the preceding example was catalytically hydrogenated over 10% palladium on carbon, in methanol, at room temperature and 1 atmosphere. The title compound was obtained, in 97% yield, as a pale-yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273999 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-5b5810871a0541ad95675a2bfe3d0994 |
| Source note | uspto-grants-1993_12 |