Benzylamine → HCID 86734615, compound

HRID 328093Notes

Reaction equation

HRID 328093 reaction equation
C(N)C1C=CC=CC=1.C(OC([NH:19][C@H:20]([C:28]([NH:30][C@H:31]([C:33]([NH:35][O:36][P:37]([CH3:40])(=[O:39])[OH:38])=[O:34])[CH3:32])=[O:29])[CH2:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)=O)C1C=CC=CC=1>>[NH2:19][C@H:20]([C:28]([NH:30][C@H:31]([C:33]([NH:35][O:36][P:37]([CH3:40])(=[O:38])[OH:39])=[O:34])[CH3:32])=[O:29])[CH2:21][C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 86734616HCID 86734616, compound

Product 1

HCID 86734615HCID 86734615, compound

Procedure

In a manner analogous to that given in Example 7 (b), from the benzylamine salt of [(N-benzyloxycarbonyl-L-phenylalanyl-L-alanyl)amino]-methylphosphonic acid there was obtained (L-phenylalanyl-L-alanylamino)-methylphosphonic acid of melting point 262°-264° C (decomposition); [α]D20 = - 9.6° (c = 0.5% in water).

Sources & evidence

ORD record
ord-f9b2b9d7e46442c796d4f96365352dd6
Source dataset
uspto-grants-1977_04
Patent number
US04016148

Reaction notes

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