Chloroacetone → HCID 54056857, compound

HRID 328099Notes

Reaction equation

HRID 328099 reaction equation
[NH:1]([C:3]1[CH2:9][N:8]=[C:7]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=2[Cl:16])[C:6]2[CH:17]=[CH:18][CH:19]=[CH:20][C:5]=2[N:4]=1)[NH2:2].[Cl:21][CH2:22][C:23](=O)[CH3:24]>>[Cl:21][CH2:22][C:23](=[N:2][NH:1][C:3]1[CH2:9][N:8]=[C:7]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=2[Cl:16])[C:6]2[CH:17]=[CH:18][CH:19]=[CH:20][C:5]=2[N:4]=1)[CH3:24]

Participants

3

Reactant 2

HCID 6571ChloroacetoneHCID 12612344HCID 12612344, compound

Product 1

HCID 54056857HCID 54056857, compound

Procedure

In the manner given in Example 1, 2-hydrazino-5-(o-chlorophenyl)-3H-1,4-benzodiazepine can be reacted with chloropropanone to give 2-[(2-chloro-1-methylethylidene)hydrazino]-5-(o-chlorophenyl)-3H-1,4-benzodiazepine.

Sources & evidence

ORD record
ord-ffdf9c4f6498426099036128c785eb7c
Source dataset
uspto-grants-1977_04
Patent number
US04016165

Reaction notes

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