HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetoxybutyraldehyde → 4-Hydroxybutyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetoxybutyraldehyde | HCID 11007927 | — |
| Reactant | 1-Oxobutan-2-yl acetate | HCID 13033921 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Hydroxybutyl acetate | HCID 10103209 | 99% |
Reaction Steps
The procedure in Example 1 was followed but instead of the acetoxybutyraldehyde isomer mixture, 4-acetoxybutyraldehyde was employed and the hydrogenation was carried out in the presence of 5% by weight of methanol. After a hydrogenation time of 35 minutes, and after filtering off the catalyst and freeing the filtrate from methanol, 4-acetoxybutan-1-ol was obtained in 99% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04016201 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-5a77d5eeaf954d63b3f9fd6794c56a34 |
| Source note | uspto-grants-1977_04 |