HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Formyl-2-methylethyl acetate → 3-Acetoxy-2-methylpropan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Formyl-2-methylethyl acetate | HCID 10986249 | — |
| Reactant | 4-Acetoxybutyraldehyde | HCID 11007927 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Acetoxy-2-methylpropan-1-ol | HCID 10374500 | 99% |
Reaction Steps
The procedure in Example 4 was followed except that 3-acetoxy-2-methylpropionaldehyde was hydrogenated in place of 4-acetoxybutyraldehyde, in the presence of 5% by weight of methanol. After a hydrogenation time of 30 minutes and after working up as described in Example 4, pure 3-acetoxy-2-methylpropan-1-ol was obtained in 99% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04016201 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-f812a10b4507427bb3e1d6d70e5bb6f1 |
| Source note | uspto-grants-1977_04 |