HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21444454, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 3,5-Dimethyl-4-[(pyridin-2-yl)sulfanyl]phenol | HCID 21444456 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 21444454 | HCID 21444454 | — |
Reaction Steps
4-(2-Pyridylthio)-3,5-dimethylphenol (161 g.), prepared in part A, and methylisocyanate (48 g.) was dissolved in dry toluene (1500 ml.) containing triethylamine (10 ml.) and the mixture was then stirred under reflux overnight. Further quantities of methyl isocyanate (22 g.) and triethylamine (10 ml.) were then added and refluxing was continued for a further 6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04016278 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-f3409fc254964ee69152ca37335f6d2d |
| Source note | uspto-grants-1977_04 |