Lauric acid diethanolamide → 2-[dodecanoyl-[2-(furan-2-carbonyloxy)ethyl]amino]ethyl furan-2-carboxylate

HRID 328426Notes

Reaction equation

HRID 328426 reaction equation
[OH:1][CH2:2][CH2:3][N:4]([CH2:18][CH2:19][OH:20])[C:5](=[O:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[O:21]1[CH:25]=[CH:24][CH:23]=[C:22]1[C:26](Cl)=[O:27]>>[O:21]1[CH:25]=[CH:24][CH:23]=[C:22]1[C:26]([O:1][CH2:2][CH2:3][N:4]([CH2:18][CH2:19][O:20][C:26]([C:22]1[O:21][CH:25]=[CH:24][CH:23]=1)=[O:27])[C:5](=[O:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:27]

Participants

3

Reactant 2

HCID 8430Lauric acid diethanolamideHCID 682422-Furancarbonyl chloride

Product 1

HCID 3216912-[dodecanoyl-[2-(furan-2-carbonyloxy)ethyl]amino]ethyl furan-2-carboxylate

Procedure

N,N-bis(2-furoyloxyethyl)lauramide was prepared by the procedure of example 1 from 28 gms. (0.1 mole) of N,N-bis(2-hydroxyethyl)lauramide and 26 gms. (0.2 mole) of furoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

  1. customN,N-bis(2-furoyloxyethyl)lauramide was prepared by the procedure of example 1 from 28 gms

Sources & evidence

ORD record
ord-79577e80a12d434d9b3b6e087b3a1d56
Source dataset
uspto-grants-1977_04
Patent number
US04017522

Reaction notes

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