Lauric acid diethanolamide → 2-[2-(2,2-dimethylpropanoyloxy)ethyl-dodecanoylamino]ethyl 2,2-dimethylpropanoate

HRID 328427Notes

Reaction equation

[OH:1][CH2:2][CH2:3][N:4]([CH2:18][CH2:19][OH:20])[C:5](=[O:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH3:21][C:22]([CH3:27])([CH3:26])[C:23](Cl)=[O:24]>>[CH3:21][C:22]([CH3:27])([CH3:26])[C:23]([O:1][CH2:2][CH2:3][N:4]([CH2:18][CH2:19][O:20][C:23](=[O:24])[C:22]([CH3:27])([CH3:26])[CH3:21])[C:5](=[O:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:24]

Participants

Reactant 2

HCID 8430Lauric acid diethanolamide

HCID 62493Pivaloyl chloride

Product 1

HCID 4304222-[2-(2,2-dimethylpropanoyloxy)ethyl-dodecanoylamino]ethyl 2,2-dimethylpropanoate

Procedure

N,N-bis(2-trimethylacetoxyethyl)lauramide was prepared by the procedure of example 1 from 29 gms. (0.1 mole) of N,N-bis(2-hydroxyethyl)lauramide and 24 gms. (0.2 mole) of trimethylacetyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

customN,N-bis(2-trimethylacetoxyethyl)lauramide was prepared by the procedure of example 1 from 29 gms

Sources & evidence

ORD record: ord-72d90f353b3745c88dffc52b0518eb05
Source dataset: uspto-grants-1977_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04017522

Reaction notes

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