4-Methylbenzoyl Chloride → HCID 21441865, compound

HRID 328433Notes

Reaction equation

HRID 328433 reaction equation
[CH3:1][N:2]([CH2:16][CH2:17][OH:18])[C:3](=[O:15])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[C:19]1([CH3:28])[CH:24]=[CH:23][C:22]([C:25](Cl)=[O:26])=[CH:21][CH:20]=1>>[CH3:1][N:2]([CH2:16][CH2:17][O:18][C:25]([C:22]1[CH:23]=[CH:24][C:19]([CH3:28])=[CH:20][CH:21]=1)=[O:26])[C:3](=[O:15])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

3

Reactant 2

HCID 134054-Methylbenzoyl ChlorideHCID 11737000Dodecanamide, N-(2-hydroxyethyl)-N-methyl-

Product 1

HCID 21441865HCID 21441865, compound

Procedure

N-methyl-N-(2-p-toluoyloxyetyl)lauramide was prepared by the procedure of example 1 from 26 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)lauramide and 15 gms. (0.1 mole) of p-toluoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

  1. customN-methyl-N-(2-p-toluoyloxyetyl)lauramide was prepared by the procedure of example 1 from 26 gms

Sources & evidence

ORD record
ord-a8d0f98fe7dd48549816746682477943
Source dataset
uspto-grants-1977_04
Patent number
US04017522

Reaction notes

Loading…