Pivaloyl chloride → 2-[dodecanoyl(methyl)amino]ethyl 2,2-dimethylpropanoate

HRID 328434Notes

Reaction equation

HRID 328434 reaction equation
[CH3:1][N:2]([CH2:16][CH2:17][OH:18])[C:3](=[O:15])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[CH3:19][C:20]([CH3:25])([CH3:24])[C:21](Cl)=[O:22]>>[CH3:1][N:2]([CH2:16][CH2:17][O:18][C:21](=[O:22])[C:20]([CH3:25])([CH3:24])[CH3:19])[C:3](=[O:15])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

3

Reactant 2

HCID 62493Pivaloyl chlorideHCID 11737000Dodecanamide, N-(2-hydroxyethyl)-N-methyl-

Product 1

HCID 4304242-[dodecanoyl(methyl)amino]ethyl 2,2-dimethylpropanoate

Procedure

N-methyl-N-(trimethylacetoxyethyl)lauramide was prepared by the procedure of example 1 from 26 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)lauramide and 12 gms. (0.1 mole) trimethylacetyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

  1. customN-methyl-N-(trimethylacetoxyethyl)lauramide was prepared by the procedure of example 1 from 26 gms

Sources & evidence

ORD record
ord-2117613b75de49b4965d76d162deb2b0
Source dataset
uspto-grants-1977_04
Patent number
US04017522

Reaction notes

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