Pivaloyl chloride → HCID 86734639, compound

HRID 328436Notes

Reaction equation

[CH3:1][N:2]([CH2:22][CH2:23][OH:24])[C:3](=[O:21])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10]/[CH:11]=[CH:12]\[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].[CH3:25][C:26]([CH3:31])([CH3:30])[C:27](Cl)=[O:28]>>[CH3:1][N:2]([CH2:22][CH2:23][O:24][C:27](=[O:28])[C:26]([CH3:31])([CH3:30])[CH3:25])[C:3](=[O:21])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10]/[CH:11]=[CH:12]\[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

Reactant 2

HCID 62493Pivaloyl chloride

HCID 7171990935627-93-1

Product 1

HCID 86734639HCID 86734639, compound

Procedure

N-methyl-N-(2-trimethylacetoxyethyl)oleamide was prepared by the procedure of example 1 from 34 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)oleamide and 12 gms. (0.1 mole) trimethylacetyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Workup

customN-methyl-N-(2-trimethylacetoxyethyl)oleamide was prepared by the procedure of example 1 from 34 gms

Sources & evidence

ORD record: ord-b6528995cbc64fb4ab717a91a2725787
Source dataset: uspto-grants-1977_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04017522

Reaction notes

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